Microstructure and Antibacterial Properties of Chitosan-Fe3O4-AgNP Nanocomposite

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Hartati Hartati, Subaer Subaer, Hasri Hasri, Teguh Wibawa, Hasriana Hasriana

2022 Nanomaterials Vol. 12 Issue 20 Article Cited by 19 Quartile

Abstract

The goal of this research is to synthesize and characterize Fe3O4@Chitosan-AgNP nanocomposites in order to determine their antibacterial activity. The research methods include the synthesis of Fe3O4@Chitosan-AgNP nanocomposites, as well as the characterization of nanoparticles using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared (FTIR) analysis, and subsequent antibacterial activity tests. The study’s findings demonstrated the successful synthesis of Fe3O4@Chitosan-AgNP nanocomposites, followed by nanoparticle characterization using SEM, TEM, XRD, and FTIR. Based on the XRD results, the conjugation of Fe3O4@Chitosan-AgNP nanocomposites has been successfully formed, as evidenced by the appearance of characteristic peaks of Fe3O4, chitosan, and AgNPs. According to the FTIR results, the interaction between chitosan-AgNPs and conjugated Fe3O4 occurred via the N atom in the NH2 group and the O atom in the OH group, and C=O. The SEM and TEM images also show that the Fe3O4@Chitosan-AgNP conjugation is a nanoparticle-based composite material. The combination of nanocomposites Fe3O4@Chitosan-AgNPs has antibacterial activity, inhibiting the growth of bacteria such as Bacillus cereus and Escherichia coli. © 2022 by the authors.

Affiliations

Biology Department, Faculty of Mathematics and Natural Science, Universitas Negeri Makassar, Makassar, 90222, Indonesia; Green of Excellence of Green Materials & Technology (CeoGM-Tech) FMIPA, Universitas Negeri Makassar, Makassar, 90222, Indonesia; Physics Department, Faculty of Mathematics and Natural Science, Universitas Negeri Makassar, Makassar, 90222, Indonesia; Chemistry Department, Faculty of Mathematics and Natural Science, Universitas Negeri Makassar, Makassar, 90222, Indonesia